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1 article(s) from Parracho, Ana I R

From discovery to production: Scale- out of continuous flow meso reactors

Peter Styring and
Ana I. R. Parracho

Beilstein J. Org. Chem. 2009, 5, No. 29, doi:10.3762/bjoc.5.29

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Graphical Abstract

Scheme 1: Synthesis of 4-methoxybiphenyl (4-MeOBP) and by-products in the Kumada reaction.

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Figure 1: Stainless steel single column flow reactor for discovery scale synthesis.

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Figure 2: (a): Schematic diagram of the parallel reactor housing (dimensions in mm); (b) the stainless steel ...

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Figure 3: Schematic diagram of the pneumatic pumping system.

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Scheme 2: Proposed catalytic cycles for the transformation of 4-haloanisole (Ar-X) and Grignard reagent (RMgX...

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Figure 4: Comparative study of flow rates in a single channel meso flow reactor. The output was sampled hourl...

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Figure 5: Kumada reaction carried out in a parallel channel meso reactor at a flow rate of 95 ml h⁻¹.

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Figure 6: Kumada reaction carried out in a parallel channel meso reactor over a 31-hour period at a flow rate...

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Figure 7: Kumada reaction carried out in a parallel channel meso reactor at a flow rate of 190 ml h⁻¹.

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Published 09 Jun 2009

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